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A Rapid Microwave Induced Synthesis of Isonicotinamide Derivatives and their Antifungal Activity
Croatica Chemica Acta, 92 (2019), 1; 125-135. https://doi.org/10.5562/cca3527
Bušić, Valentina; Vrandečić, Karolina; Siber, Tamara; Roca, Sunčica; Vikić Topić, Dražen; Gašo Sokač, Dajana

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Bušić, V., Vrandečić, K., Siber, T., Roca, S., Vikić Topić, D. i Gašo Sokač, D. (2019). A Rapid Microwave Induced Synthesis of Isonicotinamide Derivatives and their Antifungal Activity. Croatica Chemica Acta, 92. (1), 125-135. doi: 10.5562/cca3527

Bušić, Valentina, et al. "A Rapid Microwave Induced Synthesis of Isonicotinamide Derivatives and their Antifungal Activity." Croatica Chemica Acta, vol. 92, br. 1, 2019, str. 125-135. https://doi.org/10.5562/cca3527

Bušić, Valentina, Karolina Vrandečić, Tamara Siber, Sunčica Roca, Dražen Vikić Topić i Dajana Gašo Sokač. "A Rapid Microwave Induced Synthesis of Isonicotinamide Derivatives and their Antifungal Activity." Croatica Chemica Acta 92, br. 1 (2019): 125-135. https://doi.org/10.5562/cca3527

Bušić, V., et al. (2019) 'A Rapid Microwave Induced Synthesis of Isonicotinamide Derivatives and their Antifungal Activity', Croatica Chemica Acta, 92(1), str. 125-135. doi: 10.5562/cca3527

Bušić V, Vrandečić K, Siber T, Roca S, Vikić Topić D, Gašo Sokač D. A Rapid Microwave Induced Synthesis of Isonicotinamide Derivatives and their Antifungal Activity. Croatica Chemica Acta [Internet]. 28.01.2019. [pristupljeno 17.11.2024.];92(1):125-135. doi: 10.5562/cca3527

V. Bušić, K. Vrandečić, T. Siber, S. Roca, D. Vikić Topić i D. Gašo Sokač, "A Rapid Microwave Induced Synthesis of Isonicotinamide Derivatives and their Antifungal Activity", Croatica Chemica Acta, vol. 92, br. 1, str. 125-135, Siječanj 2019. [Online]. Dostupno na: https://urn.nsk.hr/urn:nbn:hr:151:435023. [Citirano: 17.11.2024.]

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Naslov (engleski)A Rapid Microwave Induced Synthesis of Isonicotinamide Derivatives and their Antifungal Activity
AutorValentina Bušić
AutorKarolina Vrandečić
AutorTamara Siber
AutorSunčica Roca
AutorDražen Vikić Topić
AutorDajana Gašo Sokač
Autorova ustanovaSveučilište Josipa Jurja Strossmayera u Osijeku
Fakultet agrobiotehničkih znanosti Osijek
(Zavod za fitomedicinu)
Znanstveno / umjetničko
područje, polje i grana		BIOTEHNIČKE ZNANOSTI
Poljoprivreda (agronomija)
Fitomedicina
Sažetak (engleski)
Ten novel isonicotinamide derivatives were prepared by quaternization reactions of isonicotinamide with methyl iodide and nine differently substituted 2 bromoacetophenones under rapid microwave irradiation of 10 minutes. The microwave preparations were significantly faster and with yields higher up to 8 times, than the preparations by conventional method. The structures of synthesized molecules were determined by one- and two dimensional NMR and IR spectroscopy, mass spectrometry and elemental analysis. Antifungal activity of all compounds was tested in two different concentrations (10 and 100 µg mL–1) against Fusarium oxysporum, Fusarium culmorum, Macrophomina phaseolina and Sclerotinia sclerotiorum in vitro. From the antifungal assay it can be seen that the most prepared compounds have moderate to weak activity against M. phaseolina and F. culmorum. A very high inhibitory rate was observed against S. sclerotiorum, 62–87.5 % in concentration of 10 µg mL–1 and 83.7–93.2 % in concentration of 100 µg mL–1. <br><a rel="license" href="http://creativecommons.org/licenses/by/4.0/"><img alt="Creative Commons License" style="border-width:0" src="https://i.creativecommons.org/l/by/4.0/80x15.png" /></a> This work is licensed under a <a rel="license" href="http://creativecommons.org/licenses/by/4.0/">Creative Commons Attribution 4.0 International License</a>.
Ključne riječi (engleski)
Jezikengleski
Vrsta publikacijeZnanstveni rad - Izvorni znanstveni rad
Status objaveObjavljen
Vrsta recenzijeRecenziran - domaća recenzija
Verzija publikacijeObjavljena verzija rada (izdavačev PDF)
Naslov časopisaCroatica Chemica Acta
Brojčani podacivol. 92, br. 1, str. 125-135
p-ISSN0011-1643
e-ISSN1334-417X
DOIhttps://doi.org/10.5562/cca3527
URN:NBNurn:nbn:hr:151:435023
Datum objave publikacije2019-01-28
URL dokumentahttps://hrcak.srce.hr/222767
Vrsta resursaTekst
Prava pristupaOtvoreni pristup
Uvjeti korištenjaIkona licence Zaštićeno autorskim pravom.
Datum i vrijeme pohrane2024-06-27 10:34:23